Syllabus

CHE 515 X-Ray Diffraction (3-0)3

Fall 2010

Diffraction theory and its relationship to structural determination in solids,

focuses on applications of X-rays.

 

Course Instructor

Sedat Akkurt, PhD

Professor

Office: 108 Mechanical Engineering

Phone: (232) 750-6705

e-mail: sedatakkurt@iyte.edu.tr

Class Web-Page: http://www.iyte.edu.tr/~sedatakkurt/che515/che515ana.html

 

Class Hours:

Tuesdays: 1:30-3:15

Thursdays: 1:30 - 2:15 

 

Office Hours:

Wednesdays: 10:30am - 12:00am 

 

Introduction:

XRD is a tool for the investigation of the crystal structures of materials. It is an extremely important analytical tool for researchers in materials related disciplines. This class is intended to provide the students with the knowledge of X-Ray Diffraction (XRD) and its applications. We will mainly cover the following topics in this course: properties of x-rays, crystallography, geometry of crystals, diffraction and experimental methods like powder XRD and applications like crystal size, crystal structure, amorphous materials, precise parameter measurements, phase diagram determination and multiphase quantitative analysis. When you leave Iztech with your masters degrees, I want you to be "competent" in x-ray diffraction analysis of materials. I have complete faith in your goodwill and your willingness to learn. Please make me feel the same way at the end of the semester. There will be two midterm exams and a final exam in addition to several homework problems. But your performance in the labs will also be monitored. Please do not be scared by the age of the book. This is a classical book used in most of the universities worldwide. Its third edition was released but it seems like the second edition is still better. The course instructor is not meant to be a "nanny" but more like a "tour guide" in the class. It is important that we have total agreement on these matters.

 

Grading Policy:

Test

Percent Weight

Date of Test

Midterm Exam I  

25%

November 4, 2009 Thu

Midterm Exam II  

25%

December  23, 2009 Thu

Final Exam

25%

January 13, 2009 Thu 2:00pm

Homeworks

5%

 

Lab Performance and Attendance

20%

 

 

 

Lab Work:

The lab time and location will be announced later in our class web page and in the class.

 

Textbook:

B.D.Cullity, "Elements of X-Ray Diffraction", Third Edition, Addison Wesley Publishing Company, Inc., Reading, 2004.

Call Number: QC 481 C96 1978

ISBN: 0-201-01174-3

 

Course Assistants:

Mr.Erdem Þahin, Phone: 6684, erdemsahin@iyte.edu.tr

 

 

 

 

 

CHE 515 XRD Course Program for Fall 2010

Week

Subjects to be Covered

1

Introduction

2

Properties of X-rays

3

Properties of X-rays

4

Geometry of Crystals -1

5

Geometry of Crystals -2

6

Geometry of Crystals -3

7

Diffraction: Directions of Diffracted Beams

8

Diffraction: Intensities of Diffracted Beams

9

Diffraction: Intensities of Diffracted Beams

10

Applications: Crystal Structure Determination

11

Experimental Methods:Powder, Grazing Incidence

12

Wrap up

 Class location: New ME Bldg 154 (D12)

This page is last updated sept 30th, 2010  by S.Akkurt.